Li2O-MgO-Al2O3-SiO2系高温低膨胀釉的制备及性能研究

以焦炉炉门堇青石衬砖的使用情况为依据，得出适合堇青石衬砖高温低膨胀釉的体系为Li2O-MgO-Al2O3-SiO2系。釉料在合理的化学组成范围内生成堇青石与口．锂辉石固溶体晶体。试验成功的研制出适用于堇青石衬砖的高温低膨胀釉，釉料在1350℃与堇青石砖共同烧成，釉层能均匀光滑的铺展在堇青石衬砖表面，它能在1200℃下使用而不融化，它的热膨胀系数为2．85×10^-4，在20℃～1000℃并且还有待于进一步降低。釉与堇青石衬砖热膨胀相匹配，因此釉层经五次热震（1100℃，水冷）后的没有裂纹出现。XRD物相分析得出釉有堇青石与口．锂辉石固溶体晶体相生成。釉能填充堇青石衬砖表面的气孔并以自身的高致密性防止了有害物质向砖内部渗透，起保护层作用。     

高强韧性热作模具钢SDH2的研究

在高温、高压强条件TH13钢通常出现早期失效，而传统的3Cr2W8V钢却表现出韧性不足，为此通过降低Cr含量、提高Mo和V含量，添加W元素来改善热作模具钢的综合性能，设计出了SDH2钢。室温和高温冲击韧度试验、回火稳定性试验和热疲劳试验表明，1100℃淬火＋600℃回火的SDH2钢室温下冲击值大于300J；回火温度从560℃升高到625℃保温18h，SDH2钢的硬度值依然大于46HRC；另外，SDH2钢具有比H13钢更优良的抗热疲劳性能。     

变质处理高速钢导辊的研究

通过调整高速钢成分和采用RE—K—Na复合变质处理；改变了共晶碳化物的形态和分布，使铸造高速钢冲击韧度提高69．9％，热疲劳抗力也明显改善。变质处理高速钢导辊使用中不粘钢、不破碎、不剥落，使用寿命比高镍铬合金铸钢和Crl2MoV锻钢导辊提高2—3倍。     

Effect of copper addition on the thermal contraction of indium melt clusters

The structure of In-1%Cu and In-5%Cu (mass fraction) alloy melts were studied at different temperatures above liquidus by using a high-temperature X-ray diffractometer and were compared with that of pure In melt. Experimental results show that with the addition of 1% Cu or 5% Cu, the thermal contraction phenomenon of atom clusters occurs in melts with the temperature increasing like pure In melt. With the addition of 1% Cu, the thermal contraction of atom clusters increases and the contraction is not homogeneous in the whole measurement temperature range. The sudden change and noticeable contraction can be found in the range of 280-390℃. The temperature range of the sudden change is lower than that of pure In melt. With the addition of 5% Cu, the thermal contraction of atom clusters decreases and the contraction is not consistent in the whole measurement temperature range. The anomalous change can be measured at about 600 ℃. At the same superheating temperature, the nearest interatomic distance r1 of     

稀土对复合处理渗层热疲劳性能的影响

进行了稀土对４Ｃｒ５ＭｏＳｉＶｌ钢硫氮碳共渗加氧化复合处理渗层热疲劳性能影响的研究结果表明，添加稀土的渗层比未添加稀土的热疲劳性能有显著提高。     

Technical note: Plasma-sprayed ceramic thermal barrier coatings for smooth intermetallic alloys

A durable ceramic thermal barrier coating is applied directly to a smooth, highly oxidation resistant intermetallic alloy in two layers. The first layer of ceramic is applied by low pressure plasma spraying and the second layer is applied by conventional atmospheric pressure plasma spraying. This approach would allow the use of plasma sprayed ceramic coatings in applications where a metallic bond coat is not desirable.     

纳米Pt膜的晶粒尺寸及其对热导率的影响

采用电子束-物理气相沉积法（EB-PVD）制备了6个厚度为15-62nm的铂薄膜，研究了纳米薄膜的晶粒尺寸及其对热导率的影响规律．当薄膜厚度小于30nm时，晶粒平均尺寸接近于薄膜的厚度；晶粒尺寸随着薄膜厚度的增加而增大并趋于定值；当薄膜厚度大于30nm时，晶粒尺寸约为20nm．受薄膜的表面和内部晶界的综合影响，铂纳米薄膜的热导率大大低于体材料的值，并且纳米薄膜的热导率随着薄膜厚度的增加而增大并趋于一个低于体材料热导率的值．     

铜合金表面Ni基铸渗层的热疲劳行为研究

研究了铜基表面镍基渗层的热疲劳性能。结果表明:热循环次数小于20次时,渗层表面主要产生氧化,无裂纹产生;当热循环次数超过50次时,渗层与基体的结合界面处以及渗层的表面会产生微裂纹,渗层越厚,渗层与基体的结合界面处出现微裂纹的时间越早;多次热循环后在渗层与基体的结合处出现蚀坑,渗层的损伤形式主要为应力腐蚀。     

炼铁原、燃料检、实验系统的建立与应用

介绍了济钢炼铁原、燃料检、实验系统的构成，主要性能特点，使用过程中的经验教训。此系统使用后年节省检、实验费用95．64万元。     

Graded plasma spraying of premixed metalceramic powders on metallic substrates

The mismatch between the thermal expansion coefficients of ceramics and metals and the differential stresses it causes at the interface create problems in metal to ceramic joining. Research has been con-ducted to solve this problem in thermal barrier coating technology. Previous studies have considered met-al-ceramic multilayers or graded-coatings, which include a metallic bond coat. In this study, a graded plasma-sprayed metal-ceramic coating is developed using the deposition of premixed metal and ceramic powders without the conventional metallic bond coat. Influences of thickness variations, number, and composition of the layers are investigated. Coatings are prepared by atmospheric plasma-spraying on In-conel 718 superalloy substrates. Ni-Cr-Al and ZrO₂ -8 % Y₂O₃ powders are used for plasma spraying. Ad-hesive and cohesive strength of the coatings are determined. The concentration profile of the elements is determined by x-ray energy-dispersive analysis. The microstructure and morphology of the coatings are investigated by optical and scanning electron microscopy (SEM). Results show that the mixed metal-ce-ramic coating obtained with the deposition of premixed powders is homogeneous. The morphology and microstructure of the coatings are considered satisfactory.